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Beilstein J. Org. Chem. 2022, 18, 1133–1139, doi:10.3762/bjoc.18.117
Graphical Abstract
Figure 1: Structures of chitin and chitosan oligosaccharides.
Figure 2: Effect of the anomeric leaving group on the yield of oligosaccharides.
Figure 3: Influence of the glycosylation temperature (T2) on the yield of oligosaccharides.
Figure 4: Influence of temperatures of anodic oxidation (T1) and glycosylation (T2).
Figure 5: MALDI–TOF MS spectra of oligosaccharides.
Figure 6: Proposed structures of byproducts of electrochemical polyglycosylation.
Figure 7: Proposed mechanisms of electrochemical polyglycosylation.
Figure 8: Oxidative potential of monosaccharide 1a, disaccharide 2a, and trisaccharide 3a.
Scheme 1: Electrochemical dimerization of tetrasaccharide 4a.
Figure 9: Influence of cycle number on the yield of longer oligosaccharides 5a (n = 5)–8a (n = 8). Conditions...
Beilstein J. Org. Chem. 2017, 13, 919–924, doi:10.3762/bjoc.13.93
Figure 1: Inhibitors of glucosaminidases.
Scheme 1: Synthesis of disaccharide donors.
Figure 2: Proposed mechanism and origin of the selectivity.
Figure 3: Synthesis of TMG-chitotriomycin precursor 7.
Figure 4: Synthess of TMG-chitotriomycin (1).